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Meeting Materials Science & Technology 2011
Symposium Recent Advances in Structural Characterization of Materials
Presentation Title Atom-Scale Characterization of the Chemistry and Structure of Material Transfer onto AFM Tips Resulting from Nanoscale Contact and Sliding Experiments
Author(s) Christopher J Tourek, Sriram Sundararajan
On-Site Speaker (Planned) Sriram Sundararajan
Abstract Scope While atomic force microscopy (AFM) based techniques have proved very useful in investigating nanotribological phenomena, a detailed assessment of the material structure and chemistry of the near apex region of the AFM tip can provide further insights. Specific areas that would directly benefit from this information include fabrication and friction/wear studies using AFM tips where material transfer and tip chemistry are of importance. Few techniques exist that can provide this critical information. We present our investigations utilizing atom probe tomography to successfully study the near apex regions of an AFM tip at the atomic scale. Further we report our initial observations on the formation of transferred material during dry sliding experiments involving a commercially available Si AFM tip on Cu. The effects of sliding distance and normal load on the formation of transferred material are also reported. The technique opens up a new avenue of investigation for AFM-related materials research.
Proceedings Inclusion? Definite: A CD-only volume

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A Multiple Partial Unloading Indentation Technique for Elastic-Plastic Mechanical Property Evaluation: Numerical and Experimental Investigation
A Novel Multi-Modal 3D Characterization System to Quantify Grain-Level Microstructural Features in Macro-Scale Volumes
Advanced Characterization of the Helical Growth of Dendritic Structures in Synthetic and Naturally Occurring Magma
Atom-Scale Characterization of the Chemistry and Structure of Material Transfer onto AFM Tips Resulting from Nanoscale Contact and Sliding Experiments
Concurrent Raman and Brillouin Scattering for Monitoring Polymer Network Assembly
Crystal Structure and Surface Analysis of Diamond-Like Semiconductor Single Crystals
Deformation in FCC Copper, Experiment and Simulation
Full-Speed Simultaneous EBSD and Spectral Image EDS Acquisitions
High-Energy X-Ray Tomography on 3D Microporous Composite Anode of Lithium-Ion Batteries
In-Situ Analysis of Deformation and Recrystallization Mechanisms in Magnesium Alloys
In Situ Studies on the Effect of Oxygen Partial Pressure on Ferroelectric Thin Films
Large Scale EBSD Collection and Analysis
Microscopic Surface Mapping of the Thermal Diffusivity by Photothermal Confocal Defocusing
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Recent Advances in APT Characterization of Nanoclusters and Nanovoids
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Rietveld Refinement of an Oil Field Cement Blend
Solid State Nuclear Magnetic Resonance Spectroscopy of Ordered and Disordered Materials
Stress Partitioning Behavior in BCC/FCC Multilayered Steels Measured by In Situ Neuron Diffraction during Tensile Deformation
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