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Meeting Materials Science & Technology 2017
Symposium Processing and Performance of Materials Using Microwaves, Electric and Magnetic Fields, Ultrasound, Lasers, and Mechanical Work – Rustum Roy Symposium
Presentation Title Evolution of Distinct Phase Composition in TiO2 Thin Films Grown under Electromagnetic Excitation
Author(s) Nathan Nakamura, Maxwell W Terban, Simon J.L. Billinge, B. Reeja Jayan
On-Site Speaker (Planned) Nathan Nakamura
Abstract Scope The application of electromagnetic (EM) fields, specifically microwave radiation (MWR), during material synthesis can promote rapid, low temperature material growth. We utilize synchrotron x-ray radiation and the thin film pair distribution function analysis technique (tfPDF) to show that MWR enables single-step synthesis of mixed amorphous-crystalline titanium dioxide (TiO<SUB>2</SUB>) films and achieves crystallinity at significantly reduced reaction temperatures and times. More importantly, our experiments demonstrate that films grown by MWR-assisted synthesis contain a different phase composition and increased crystallinity compared to TiO<SUB>2</SUB> grown at similar temperatures without EM field exposure. MWR-grown films are composed of a mixed-phase structure consisting of long-range anatase TiO<SUB>2</SUB> with short-range amorphous components, while furnace-grown materials are amorphous with local ordering most resembling the brookite phase of TiO<SUB>2</SUB>. These results indicate a clear influence of MWR on lattice formation, and can have important implications for EM field-assisted phase transformations and material growth.
Proceedings Inclusion? Undecided

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

2.45 GHz Hybrid Microwave Crystallization of LAGP Solid-state Electrolyte
A Study of Heavy Clay Body Properties for Hybrid Microwave Firing
Average Permittivity and Microwave Heating Characteristics of Electric Conductor and Insulator (Dielectrics) Mixtures
Characterization and Modeling of Epoxy Resin Reaction Kinetics by Use of In-situ Dielectric Measurements
Effect of Density and Crystallization on the Hardness of Spark Plasma Sintered Fe – based Bulk Amorphous Alloy
Effect of Plastic Deformation on L1₀ Chemical Ordering and Microstructure of Equiatomic FePd
Effect of Zn Substitution on Bi1.6Pb0.4Sr2Ca2Cu3-x ZnxO10 Thin Films Prepared by Pulsed Laser Deposition.
Effects of DC Electric Fields on Crystallization and Grain-growth in BaTiO3 Thin Films
Effects of Elastic Waves at Several Frequencies on Biofilm Formation in Circulating Laboratory Biofilm Reactors
Electric Field-assisted Pressureless Sintering Zirconia-Scandia-Ceria Solid Electrolytes
Energy and Productivity Potential of Electrotechnologies in Industrial Process Heating Systems
Evolution of Distinct Phase Composition in TiO2 Thin Films Grown under Electromagnetic Excitation
Experimental Analysis for Thermally Non-equilibrium under Microwave Irradiations to Oxide Iron Powders
Grain Refinement of Ni-based Superalloy under Magnetic-thermal Coordinated Control
In Situ Study of Lattice Expansion during Flash Sintering
Influence of Applied Magnetic Fields on Rare-earth & Transition Metal Dopants in α-Al2O3
Investigation of Microwave Solid State Synthesis of Highly Ordered Structures
Investigation of Single- mode Microwave Coupling in SiC-TiB2 Materials
J-54: Microstructure and Texture of Electromagnetic Formed OFHC Copper and Glidcop Al-15
Mechanistic Insights into Low Temperature Ceramic Thin Film Growth and Crystallization Using Microwave Radiation
Microwave-augmented Crystallization and Decrystallization in Ceramic Processing -- A Phenomenology-Based Commentary
Microwave Joining Process of an Aluminosilicate Ceramic Material for Radioactive Waste Containers
Microwave Pyrolysis of Pine Sawdust for Preparation of Highly Porous Biochar
Microwave Technology for Commercial Scale Processing of Ceramic Materials
Monika Willert-Porada Memorial Lecture: Microwave Processing from Fundamentals to Application
Observation of Re-entrant Spin Reorientation in TbFe1-xMnxO3
Observations on the Effect of Electric Field on Mullite Formation in Porcelains
Porous Ceramic/Metal Composite Body for DPF (Diesel Particulate Filter) and the Microwave Heating Behavior
Recrystallization and Grain Growth of Electromagnetic Formed OFHC Copper and Glicop Al-15
Resilient Graphitic Carbons from Electro-thermal Fluidized Bed Reactor
Room Temperature Magnetic Processing of Advanced Ceramics
Sinter-forging and Spark Plasma Sintering of WC-Co for Enhanced Mechanical Properties
Structure and Properties of Microwave-consolidated Magnesium Powders
Ultrafast Laser Processing of Ceramics and Glasses
Ultrasonic Energy Enabled Dynamic Recovery in Aluminium during Micro Forming and Its Effects on Stress and Microstructure Evolution
Understanding the Mechanism of Flash Sintering with In Situ EDXRD Experiments
Variable Frequency Microwave (VFM) Processing of Battery Electrodes

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