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Meeting 2010 TMS Annual Meeting & Exhibition
Symposium General Poster Session
Presentation Title Step-Wise Exothermic Reactions in Cold-Rolled Ni/Al, Ti/Al, and Ta/Al Multilayer Foils
Author(s) Laszlo J. Kecskes, Anthony J Roberts, Nathan R Wingate, Bradley R Klotz, Xiaotun Qiu, Jiaping Wang
On-Site Speaker (Planned) Laszlo J. Kecskes
Abstract Scope Exothermic reactions in cold-rolled Ni/Al, Ti/Al, and Ta/Al reactive multilayer foils were investigated. To understand conditions approaching combustion synthesis reactions, the cold-rolled samples were heated to temperatures above 1000 C in a differential scanning calorimeter. During heating, a series of endo- or exothermic peaks were noted; corresponding to a multi-step process, the relative positions, widths, and amplitudes of the peaks were found to be indicative of a stepwise reaction. Subsequent to obtaining the total calorimetric heat output for a given heating rate, samples were also heated to each peak temperature to identify the intermediate reaction product and evolution of the microstructure from reactants to steady state products. Scanning electron microscopy showed that lower temperature peaks corresponded to aluminum-rich intermetallics, while higher temperature peaks corresponded to conversion of these intermetallics to the nominal composition. Differences in the stepwise reaction mechanisms, as dictated by the underlying intermixing processes, are described.
Proceedings Inclusion? Definite: A CD-only volume

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