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Meeting 2010 TMS Annual Meeting & Exhibition
Symposium Coatings for Structural, Biological, and Electronic Applications
Presentation Title Method of Characterizing Pore Structure in Porous Coating Layer using a Simple Voltammetry
Author(s) Nancy L. Michael, Woong-Ho Bang, Choong-Un Kim
On-Site Speaker (Planned) Nancy L. Michael
Abstract Scope Porous thin films are used in various applications, including the coating for biomaterials and energy storage materials, as they provide unique electrical, structural and chemical properties that are not available at the bulk. Characterization of pore structure is typically done by a direct observation of pores using microscope, but such techniques only visualize limited volume of the film. The need for new characterization techniques is growing, especially because the use of thin films with extremely small pore size, is expanding. A new technique that can characterize the pore structure without limitations of microscopy is developed in our research. This technique is based on a simple voltammetry that uses ions in electrolyte as pore size tracer and found to work even with nanoscale pores. This paper introduces theoretical background and experimental examples of the technique.
Proceedings Inclusion? Planned: Other (describe below)

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Load-based Depth-sensing Micro-indentation Technique for Spallation Detection of Thermal Barrier Coatings
A Nucleation and Growth Model for Pulse Plated Trivalent Chromium Deposition
An Investigation on Phase Formations and Microstructures of Ni-rich NiTi Shape Memory Alloy Thin Films
Carrier Concentration Tuning and Enhanced Photoelectrochemical Response of Bandgap-Reduced Cu and Ga Co-Doped P-Type Zno Films
Crystallization and Thermal Stability of Amorphous and Nanocrystalline TiO2 Magnetron-Deposited Thin Films Studied by X-ray Diffraction
Diaphragm Coatings to Enhance Performance of Fabry-Perot Sensors
Effect of Heat Treatment on the Microstructure and Mechanical Properties of Ti-Mo-N Coating Films
Effect of Superficially Applied Y2O3 Coating on High Temperature Corrosion Behaviour of Ni-Base Superalloys
Evaluation of Thermal and Intrinsic Stress in Copper and Tantalum Sputtered Films
Experimental Study of Ternary Cobalt Spinal Oxides for Photoelectrochemical Hydrogen Production
Method of Characterizing Pore Structure in Porous Coating Layer using a Simple Voltammetry
Microstructure and Mechanical Properties of Vanadium Oxide-based Coatings on Steel Substrates Prepared by Pulsed Laser Deposition
Microstructure and Mechanical Properties of Yttria-stablized Zirconia Coatings Produced By Electrophoretic Deposition and Microwave Sintering
Molecular-scale Surface and Interfacial Coatings Utilizing Self-Assembled Monolayer of Phosphonates (SAMP) technology
Morphological Evolution during the Annealing and Growth of Polycrystalline Films
Organic Coatings to Prevent Molten Metal Explosions
Phase Change Materials – An Overview
Piezoelectric Measurements and Microstructural Characterization of ‘Smart’ AlN Thin Films Fabricated by Pulsed Closed Field Unbalanced Magnetron Sputtering
Plasma Spray Coatings for Aerospace Applications
Preparation of the Biomimetic Calcium Phosphate Coating on CoCrMo Implant Alloys via an Effective Chemical Activation
PVD Coated Hot Work Tool Steels for Tooling Applications in Semi-Solid Processing of Steels
Research on Nano Fe2O3 Film Coated on Surface of 3D-Meshwork SiC by Sol-Gel Method
Semiconductor Device Integration Utilizing Magnetic Films
Spin Coated Er-Doped SiO2 for High Efficiency Waveguide Optical Amplifiers
Stellite Coatings on Hot Work Tool Steels for Tooling Applications in Semi-Solid Processing of Steels
Surface Modification of Nanostructured Materials for Functional Medical Devices
Surface Modification of Steel Substrate by Pulsed Laser Deposition Technique
Synthesis of Amorphous Al-Co-Ce Alloys via Atomization and Mechanical Milling
Temperature and Scale Dependent Deformation and Creep Behavior of Polymer Derived Si-C-O Ceramics
The Effect of Aging Time on the Properties of Sol-Gel Derived Nanostructure Fluorapatite Powder and Coating
Using Artificial Neural Network to Optimize Thickness and Hardness of TiN Layers Deposited by PACVD Method

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