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Meeting MS&T22: Materials Science & Technology
Symposium Additive Manufacturing of High and Ultra-high Temperature Ceramics and Composites: Processing, Characterization and Testing
Presentation Title Evaluating Extrusion Deposited Additively Manufactured Fiber-reinforced Thermoplastic Polymers as Carbon/Carbon Preforms
Author(s) Edwin Romero, Eduardo Barocio, Rodney W. Trice
On-Site Speaker (Planned) Edwin Romero
Abstract Scope Extrusion deposition additive manufacturing of thermoplastic polymers allows embedded fibers to be oriented locally and globally without the use of molds, enabling more control over fiber architectures, the matrix thermal history, and its microstructure. Carbon/carbon composite processing can benefit from extrusion deposition additive manufacturing but thermoplastic conversion to carbon results were needed. In this study, we analyzed several short carbon fiber-reinforced thermoplastic polymers with varying fiber contents, including polyphenylene sulfide, polyetherimide, poly sulfone, polyether sulfone, and polyether ether ketone via thermogravimetric analysis and carbonization tests to compare carbon yields and dimensional stabilities during pyrolysis. The results showed that conversion of short carbon fiber-reinforced polyphenylene sulfide into carbon/carbon composites was the most promising because of its dimensional stability. The carbonization results for an additively manufactured fiber-reinforced polyphenylene sulfide nozzle showed that slow heating rates could be used to perform shape- and size-preserving initial pyrolysis processing of more complex geometries.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Additive Manufacturing of Chopped Fiber Ultra-High Temperature Ceramic Composites
AM of SiC:SiC Composites via Robocasting
Anisotropic Microstructures in Platelet-Seeded Silicon Carbide obtained via Direct Ink Writing
Considerations for Additive Manufacturing of Ultra-high Temperature Ceramic Composites Using Preceramic Polymers
Evaluating Extrusion Deposited Additively Manufactured Fiber-reinforced Thermoplastic Polymers as Carbon/Carbon Preforms
Heterogeneous Lattice Structure Ceramic-Refractory Metal Materials Created via Additive Manufacturing
High-temperature Performance of LCVD SiC Fiber-Reinforced CMCs
In-Bath 3D Printing of Preceramic Polymers
Laser-induced Slip Casting for Additive Manufacturing of Large Ceramic Components
Micro and Nanostructured Compositing Approaches to Green Body Strengthening of Polymer-Derived UHTC
Optimizing Functionally Graded ZrB2-Mo Components by Ceramic On-Demand Extrusion (CODE)
Oxidation Behavior of Additively Manufactured SiC-SiOC Composites
Strategies for Printing Fibers and Post-processing for Ceramic Matrix Composites (CMCs)
Structural Characterization of the 3D Printed Ceramic Composite Materials

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