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Meeting Materials Science & Technology 2019
Symposium Mechanochemical Synthesis and Reactions in Materials Science IV
Presentation Title Easy Access to Copper-antimony Mixed Sulfides (CuxSbySz): Mechanochemical Synthesis, and Structural and Surface Analysis
Author(s) Antonio F. Fuentes, Francisco A. López-Cota, Isidro J. González-Panzo, José A. Díaz-Guillén, Joelis Rodríguez-Hernández, Patricia Quintana
On-Site Speaker (Planned) Antonio F. Fuentes
Abstract Scope Mixed metal chalcogenides are an important group of functional materials for a wide-range of technological applications, mainly in the electronic and optoelectronic industry. Typically, they are synthesized by firing under vacuum, mixtures of the corresponding elemental powders, or by complex solution-mediated approaches. Herein, we show that Cu/Sb mixed sulfides, can be easily obtained under ambient conditions (air), by a simple, and convenient mechanochemical method, starting from commercially available binary sulfides (Sb2S3, Cu2S and CuS), Thus, nanometric single phase chalcostibite (CuSbS2), famatinite (Cu3SbS4), and tetrahedrite, (Cu12Sb4S13) powders, were all prepared by dry milling in a planetary ball mill, the corresponding starting mixtures. However, attempts to obtain skinnerite (Cu3SbS3) yielded a mixture of CuSbS2 and Cu12Sb4S13. As-prepared samples were characterized by XRD using the Rietveld method, thermal analysis and by XPS showing similar characteristics to analogous sulfides obtained by more elaborate powder processing methods.
Proceedings Inclusion? Planned: Other (journal publication, etc.; describe below)


A Mechanochemical Effect in Cutting of Ductile Metals
Easy Access to Copper-antimony Mixed Sulfides (CuxSbySz): Mechanochemical Synthesis, and Structural and Surface Analysis
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First Hydrogenation Characteristic of TiFe + 4wt% Zr + 2wt% Mn Alloy after Air Exposure and Reactivation by Mechanical Treatment
In-situ Synthesis of AlN-CNT Nanocomposites by Mechanochemical Reaction of Al and Melamine
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Mechanically Activated Combustion Synthesis of Nb5Si3/Nb Composites
Mechanically Activated SHS of Silicon-based Nanostructured Materials
Mechanically Alloyed Nanostructured Steels
Mechanically Driven Phase Transformation in Sn Reinforced Al-Cu-Fe Quasicrystalline Matrix Nanocomposite: Influence of Mechanical Milling and Cryomilling
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Nanocrystalline Maraging Steel Powder Fabricated by Mechanical Milling and their Thermal Stability
Neutron Total Scattering Analysis of Materials Processed by Far-from-equilibrium Methods
P2-64: Ionic Conductors Synthesized by Mechanochemistry: Exploring the ZrO2-Y2O3-Gd2O3 System.

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