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Meeting 2021 TMS Annual Meeting & Exhibition
Symposium Characterization of Materials through High Resolution Imaging
Presentation Title Magnetic Correlations and Time Fluctuations in Assemblies of Fe3O4 Nanoparticles Probed via X-rays
Author(s) Karine Chesnel
On-Site Speaker (Planned) Karine Chesnel
Abstract Scope Magnetic nanoparticles are increasingly used in biomedical applications such as drug-delivery, gene delivery, hyperthermia, or contrast agents for MRI. Magnetite (Fe3O4) nanoparticles are good candidates for these applications due to their non-toxicity and long-life in the bloodstream. Here we show inter-particle magnetic correlations probed at the nanoscale via x-ray resonant magnetic scattering (XRMS). We show the dependence on particle size, varying from 5 to 11 nm, suggesting an enhancement of magnetic couplings for bigger particles. Additionally, we show a model based on chains of nanoparticles. The data fitting suggests ferromagnetic ordering when an external magnetic field is applied, but the emergence of antiferromagnetic ordering at remanence. Additionally we will present photon correlation data that show the dynamics of fluctuation throughout the superparamagnetic blocking transition.
Proceedings Inclusion? Planned:

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Adaptive Machine Learning for 3D Bragg Coherent Diffraction Imaging Reconstructions
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Image-based Simulation of Permeability and Image-to-Mesh Conversion of X-ray Tomographic Images of a Nickel Foam
Imaging Materials on the Run: Shedding Light on Fast Structural Processes Using Time-resolved Synchrotron X-ray Tomographic Microscopy
Imaging Phase Transitions of Quantum Materials with Bragg Coherent X-ray Diffraction
Improve Phase Retrieval Performance in Bragg CDI by Simultaneous Reconstruction of Multiple Diffraction Peaks
In Situ and Operando 3D Nano-imaging for Materials Science at the ESRF
Indexing Grains: A Comparison between Three-dimensional Synchrotron X-ray Diffraction and Electron Backscatter Diffraction Techniques
Investigating the Early Life on Earth with Nanoscale X-ray Coherent Imaging
Laboratory and Synchrotron-based X-ray Tomographic Imaging during In Situ Loading of Materials
Magnetic Correlations and Time Fluctuations in Assemblies of Fe3O4 Nanoparticles Probed via X-rays
Megahertz X-ray Microscopy for Imaging High-speed Phenomena in Opaque Materials
Mesoscale Defect Dynamics in the Bulk with Time-resolved Dark-field X-ray Microscopy
Microstructural Characterization and Mechanical Behavior of a Meteorite Using Correlative Microscopy
Multi-peak Phase Retrieval for Coherent X-ray Diffraction Imaging at High Energies
Near-surface Optical Characterisation of Ion Implantation in Titanium Oxide Thin Films
Optimization Based Approach for 3D Alignment in X-ray Nano-tomography
Ptychographic Inversion with Deep Learning Network and Automatic Differentiation
Quantitative Data Analysis of Dynamic Tomography Data with Motion Artifacts
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Study of Structure of Beam-sensitive Supported Nanoparticle Catalysts by Low-dose High Resolution Phase Contrast Imaging
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Using the Rotation Vector Base Line Electron Back Scatter Diffraction (RVB-EBSD) Method to Characterize Single Crystal Cast Microstructures
X-ray Based Nanodiffraction to Study Strain in Materials for Nuclear Energy
X-ray Imaging of Three-dimensional Magnetic Systems and Their Dynamics

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