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Meeting 2019 TMS Annual Meeting & Exhibition
Symposium Characterization of Materials through High Resolution Imaging
Presentation Title Identification and Visualization of Chemical Outliers through Scientific Data Mining in Nanoscale Spectro-microscopic Study of NMC Electrode
Author(s) Enyuan Hu, Yijin Liu, Xiao-Qing Yang
On-Site Speaker (Planned) Enyuan Hu
Abstract Scope The battery electrode is structurally and chemically heterogeneous over a wide range of length scales. The heterogeneity, which could be intentionally engineered or could be formed due to anticipated/unanticipated evolution of the material upon battery operation, plays a key role in affecting the performance at device level. In this work, the chemical sensitive transmission x-ray microscopy was used to investigate NMC secondary particles that have gone through long term cycling over different voltage windows. While the overall degree of chemical heterogeneity is found to be similar in all the samples, through a machine learning approach developed herein, we identified and visualized the chemical outliers in the particles that have gone through relatively more harsh cycling condition. The formation, evolution, and migration of these chemical outliers are believed to be responsible for the capacity and voltage fade of the NMC electrode when cycled to high electrochemical potential.
Proceedings Inclusion? Planned: Supplemental Proceedings volume

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

3D Mapping of Subgrains with High Resolution 3DXRD
A Fast Algorithm for Improving Reconstruction Quality with Incomplete Tomography Data
Advances in Fatigue Crack Growth Characterization via In Situ Phase Contrast Tomography Imaging
Coherent Diffraction Imaging at High X-ray Energies
Computational Investigation of Limits of Bragg Coherent Diffraction Imaging
Deep Learning of Inverse Problems in Scanning Transmission Electron Microscopy/Scattering
Deep Neural Networks for Feature Extraction and Image Reconstruction from Coherent X-ray Diffraction Imaging Data
Deformation Behavior of Functionally Graded Polymeric Foams Using X-ray Tomography
Direct Observation of Point to Parallel Array Cu GB Segregation Behavior in Al Alloy 7075
Examining Dzyaloshinskii Domain Walls in Asymmetric Pt/Co/Ni/Ir Superlattices Using Lorentz TEM
Exploring Ion-irradiation Damage Using Bragg Coherent X-ray Imaging and 3D Transmission Electron Microscopy
Hard X-ray Coherent Diffraction Imaging Using Nanoscale Focusing Optics
High Throughput Nano-size Precipitates Characterization of Steels with Unprecedented Statistics: Transmission Kikuchi Diffraction on Extraction Replicas
Identification and Visualization of Chemical Outliers through Scientific Data Mining in Nanoscale Spectro-microscopic Study of NMC Electrode
In Situ Loading of Engineered Materials during X-ray 3D Tomographic Imaging
Investigation of Helium Precipitates in Ta(Ti)/Zr(Ti) Composites Made by Solid Metal Dealloying
K-18: High-resolution Multi-modal Imaging Capability at the Hard X-ray Nanoprobe Beamline of NSLS-II
Learning CDI Reconstructions with Backpropagation
Materials Characterisation via Optical Ptychographic Imaging: Principles and Applications
Measurements of Irradiation Induced 3D Strain Field at the Nanoscale with X-ray Bragg Coherent Diffraction Imaging
Multi-angle Bragg Projection Ptychography with Probe Retrieval
Multi-modal 3D Imaging of LiNi1-x-yMnxCoyO2 Cathode Material with Concentration-gradient
Multi-reflection Bragg Coherent Diffractive Imaging of Real-world Materials Samples
Multimodal Imaging Using Hard X-ray Speckle
Photoelastic Ptychography for Anisotropic Imaging of Optically Transparent Samples
Recent Development of Full-field X-ray Microscope at NSLS-II - A Case of Battery Research
Revealing the Growth Dynamics of Nature’s Forbidden Crystals
Sparse Dictionary Learning Methods for Coherent X-ray Diffractive Imaging
STEM Diffraction Contrast Image Simulations for Complex Dislocation Configurations
Three-dimensional Imaging of Vortex Phases in Ferroic Materials
Ultrahigh-speed X-ray Imaging for Studying Materials Structure Dynamics
Understanding Catalyst Complexity at Synchrotron Light Sources Using Hard X-ray Ptychography and Tomography
X-ray Coherent Surface Scattering Imaging for Surface 3D Imaging and Material Characterization

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