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Meeting Materials Science & Technology 2011
Symposium Recent Advances in Structural Characterization of Materials
Presentation Title High-Energy X-Ray Tomography on 3D Microporous Composite Anode of Lithium-Ion Batteries
Author(s) XIanghui Xiao, Fikile Brushett, Susanna Neuhold, Lynn Trahey, John Vaughey
On-Site Speaker (Planned) XIanghui Xiao
Abstract Scope Most commercially-available batteries utilize graphitic carbon anodes although this material has a relatively low energy storage capacity. Over the past decade, a number of alternative higher capacity anodes have been proposed, most are limited to short working lifetimes due to significant volume expansions and contractions during operation. To address this challenge, Trahey et al. developed a 3D microporous composite anode which showed promising initial performance compared to other alternative electrode materials. Unfortunately, the capacity of this novel anode material still fades after few tens of electrochemical cycling due to repeated shape changes and loss of electrical contact. We have applied synchrotron high-energy micro-tomography to monitor changes in anode structure in situ and in real time. This study will not only enable the optimization of the 3D microporous composite anodes but will also offer critical insights into the structure-activity relationships of high capacity porous materials within operating electrochemical energy storage devices.
Proceedings Inclusion? Definite: A CD-only volume

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

100 Hz Synchrotron Hard X-Ray Micro-Tomography
3D EBSD-FIB Characterization of Cold Roll Bonding Ti-Al-Nb Multilayer Sheets
A Multiple Partial Unloading Indentation Technique for Elastic-Plastic Mechanical Property Evaluation: Numerical and Experimental Investigation
A Novel Multi-Modal 3D Characterization System to Quantify Grain-Level Microstructural Features in Macro-Scale Volumes
Advanced Characterization of the Helical Growth of Dendritic Structures in Synthetic and Naturally Occurring Magma
Atom-Scale Characterization of the Chemistry and Structure of Material Transfer onto AFM Tips Resulting from Nanoscale Contact and Sliding Experiments
Concurrent Raman and Brillouin Scattering for Monitoring Polymer Network Assembly
Crystal Structure and Surface Analysis of Diamond-Like Semiconductor Single Crystals
Deformation in FCC Copper, Experiment and Simulation
Full-Speed Simultaneous EBSD and Spectral Image EDS Acquisitions
High-Energy X-Ray Tomography on 3D Microporous Composite Anode of Lithium-Ion Batteries
In-Situ Analysis of Deformation and Recrystallization Mechanisms in Magnesium Alloys
In Situ Studies on the Effect of Oxygen Partial Pressure on Ferroelectric Thin Films
Large Scale EBSD Collection and Analysis
Microscopic Surface Mapping of the Thermal Diffusivity by Photothermal Confocal Defocusing
Near-Edge Residual Stress Evaluations by Nanoindentation
Recent Advances in APT Characterization of Nanoclusters and Nanovoids
Recent developments in research on disordered materials using high energy x-ray diffraction.
Rietveld Refinement of an Oil Field Cement Blend
Solid State Nuclear Magnetic Resonance Spectroscopy of Ordered and Disordered Materials
Stress Partitioning Behavior in BCC/FCC Multilayered Steels Measured by In Situ Neuron Diffraction during Tensile Deformation
Structural Accommodation of Energy-Related Materials during Energy Conversion and Storage
Structural Characterization of Materials Using Synchrotron Based X-Ray Absorption and Scattering Techniques
Structure of Exfoliated Layered Oxides from Combined Techniques
Structure, Morphology and Oxidation State Determination of Iron-Substituted CuInS2 Materials Prepared by High-Temperature Solid-State Synthesis
Study of Correlation between Tensile Properties and Micro-Structure of TWIP Steels with Al Variation by Using In-Situ Neutron Scattering Experiments
Synchrotron X-Rays Simplified: A Rapid Access Mail-In Powder Service at the Advanced Photon Source
Tightly Packaged DNA in a Test Tube and in a Nano-Container
X-Ray Transient Absorption Spectroscopy Studies on Interfacial Electron Transfer

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