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Meeting 6th International Congress on 3D Materials Science (3DMS 2022)
Symposium 6th International Congress on 3D Materials Science (3DMS 2022)
Presentation Title In Operando 3D Characterization of Materials with Sub-15 nm Spatial Resolution Nano-tomography with the Transmission X-ray Microscope at APS
Author(s) Vincent De Andrade, Alex Deriy, Michael Wojcick, Sunil Bean, Deming Shu, Doga Gursoy, Viktor Nikitin, Francesco De Carlo
On-Site Speaker (Planned) Viktor Nikitin
Abstract Scope The TXM at beamline 32-ID of the APS at Argonne National Laboratory has been tailored for high throughput and high spatial resolution in operando nanotomography experiments. Thanks to a constant R&D effort, it emerged as a highly productive instrument, especially in the domain of Materials Science. Here, we will report recent upgrades that led the instrument to unprecedented level of performance. New optics conjugated with the enhancement of key mechanical components enabled 1 mn long tomographic acquisitions, to improve Zernike phase contrast measurement for materials like graphite and to achieve 3D spatial resolution of 13 nm, which is a record for a TXM and comparable to the resolution of the best hard X-ray ptychography microscopes. Then, we will present 3D characterization of material and systems in operando, like Portland cement formation over 10h with 1 min temporal resolution, Al-Cu alloy experiencing deformation or PGM-free electrocatalysts undergoing pyrolysis.
Proceedings Inclusion? Definite: Other

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

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3D Non-destructive Characterization of Electrical Steels for Quantitative Texture Analysis with Lab-based X-ray Diffraction Contrast Tomography (DCT).
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3D Phase Formation of 2D Materials Embedded Lunar Regolith During Sintering
3D Strength Prediction of a Two-phase Material Using Two-point Statistics
4D Nanoscale Imaging of Powder Feedstock Processing for Additive Manufacturing
A High-fidelity Analytical Model for Multi-peak Bragg Coherent Diffraction Imaging of Compact Crystalline Domains
A Novel Approach for High-resolution Phase Analysis using Hybrid Machine Learning Segmentation of Multi-modal FIB-SEM Datasets and its Application for Analysis of Next Generation Wear-resistant Coatings
A Perspective on Serial Sectioning System Technology for Structural Materials Characterization
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Achieving Large Volume Grain Statistics with Laboratory Based Diffraction Contrast Tomography
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Amorphous-crystalline Nanostructural Nd-Fe-B Permanent Magnets using Laser Powder Bed Fusion: Metallurgy and Magnetic Properties
Analysis of Fibers, Pores, and Mechanical Properties in µCT-scan of a Long Fiber-reinforced Thermoplastic
Application of 3D Characterization for Mechanical Modelling of Additively Manufactured AlSiMg
Application of a Laboratory-Based Multimodal X-ray Tomography to Study in 3D Correlations Between Grain Structure and Local Strain Distribution
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Automated 4D Reconstruction and Data-mining of Dislocation structures From In-situ TEM Experiments: Synthetic Training Data generation and Customized Deep Learning Strategies
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Calcium Oxalate Cluster Crystals Investigation of Ginseng Using Quantitative X-ray Micro-tomography
Calculating the Grain Boundary Inclination of Voxelated Grain Structures Using a Smoothing Algorithm
Casting Design Optimization using FEA Utilizing ICME Predicted Local Properties
Characterization of Microstructures and Deformation Mechanisms in Additively Manufactured 316L Stainless Steels
Combining Tomography and Scanning 3DXRD to Study Voids During Ductile Failure
Correlative Microscopy and Microstructural Characterization of Porosity Induced by Contouring in a Selective Laser Melted AA6061 Alloy
Correlative Microscopy: 3D EBSD with fs-Laser Plasma FIB-SEM
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Deep Learning-Based 3D Damage Quantification for Natural Cellular Solids
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Development of 3D EBSD Serial Sectioning Workflows for Enhanced Local Orientation Analysis
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Dictionary and Spherical Indexing of EBSD Data Sets
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Implicit Geometrical Measurement of Grain Structures with a Phase Field Representation
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In Operando 3D Characterization of Materials with Sub-15 nm Spatial Resolution Nano-tomography with the Transmission X-ray Microscope at APS
In Operando Multimodal and Multiscale Study of Degradation and Sodium Storage Process in Sodium-ion Batteries.
In Situ Heating for Laboratory-Based Nanoscale X-ray Microscopy
In Situ High Energy X-ray Diffraction Study of the Elastoplastic Transition in a Polycrystalline Metastable β Ti Alloy
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