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Meeting Materials Science & Technology 2012
Symposium Controlled Synthesis, Processing, and Applications of Structural and Functional Nanomaterials
Presentation Title Layer by Layer Assembly of SiO2/TiO2 Multilayers with Homo-/Heterogeneous Structures
Author(s) Zhenbo Xia, Kathy Lu
On-Site Speaker (Planned) Zhenbo Xia
Abstract Scope Multi-layer films of nanoparticles on solid surfaces have been studied in order to obtain different structures. However, no method, including Langmuir-Blodgett technique and chemisorption and polymer adsorption, could provide a general solution for nanoparticle assembly. In this study, a new strategy is used to assemble nanoparticle-based films using a layer-by-layer approach, which is suitable for most oxides. Carboxylic and amino functionalized oxide nanoparticle suspensions are used as precursors. These surface functionalized particles can be covalently bonded with each other via amine coupling with the help of 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDC)/n-hydroxysuccinimide (NHS). By controlling the assembly conditions and sequence precisely, SiO2/TiO2 multilayers with different combinations are assembled successfully on the silicon substrate. The particles are densely packed and the thin film is uniform. This method can be extended to other nanoparticles that have carboxylic and amino groups on the surface or those that can be modified to embody these functional groups.
Proceedings Inclusion? Undecided

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

3-D Self-Assembly of Flower-Like Particles under Microwave Irradiation and the Use of Hierarchical Particles in Water Treatment
Ceramic Micro-patterns by Soft Lithographic Molding of Nanoparticle Suspensions
Crystallography of Functional Nanomaterials
Development of a Model of Reverse Micelle Size with Electrolyte Additions
Directed Self-Assembly of Nanoparticle Array: A Platform to Make Novel Materials
Environmentally-Benign Electrochemical Method for Formation of Catalytic Metal Nanoparticles in a Chitosan Matrix
Ferromagnetic Zinc Oxide Nanoparticles Prepared by Pulsed Laser Ablation in Liquid
Floating Growth of Aligned ZnO Nanowire Arrays on Graphene in Solution for High-Performance Ultraviolet Detectors Applications
High Density Branched TiO2 Nanowire Architectures for Efficient Photocatalyzed Water Splitting
Hollow Silica Nanospheres Encapsulating Active Components Prepared Via One-Pot Sol-Gel Synthesis
Internal Reduction of Ni, Co, and Fe-Doped YSZ Characterized with SQUID Magnetometry
Iron–Nickel-Cobalt (Fe–Ni-Co) Alloy Particles Prepared by Ultrasonic Spray Pyrolysis and Hydrogen Reduction (USP-HR) Method
MICRO-CHANNELED HYDROXYAPATITE COMPONENTS BY SEQUENTIAL FREEZE DRYING AND FREE PRESSURELESS SPARK-PLASMA SINTERING
Nanostructured Composite Electrodes for High Performance Solid Oxide Fuel Cells
Phase-Field Crystal Modeling of Nanowire Growth
Polymer-Derived Si(B)CN-MWCNT Composite Coatings for High Power Laser Radiometry
Shape-Controlled Synthesis and Reactivity-Shape Correlation Study in CeO2 Nanocrytals
Solids Loading Effects on Sintering of Kaolinite-Silica Porous Composite
Sonochemical Synthesis of Cadmium Sulfide Nanoparticles
Structure and Property Relationships for CNT Turfs
Synthesis and Characterization of Nanocrystalline Nickel Zinc Oxide Particles by Ultrasonic Spray Pyrolysis
Synthesis and Chemical Characterization of SiOC-Graphene Composite Paper
Synthesis and Fabrication of Nanostructured Calcium Phosphates and their Biomedical Applications
Synthesis of Large-Area Few Layer Graphene Films by Rapid Heating and Cooling in a Modified APCVD Furnace
The Effects of Interfaces on the Ultrafast Irradiation of Thin Films
Thermally Stable Nano-grained Mg Composites Reinforced with MAX Phases
Voltage Decreasing Rate Effect during Two-Step Anodization on Multilayer TiO2 Nanotubes

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