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Meeting 2021 TMS Annual Meeting & Exhibition
Symposium Characterization of Nuclear Materials and Fuels with Advanced X-ray and Neutron Techniques
Presentation Title Multimodal Synchrotron Characterization of Transmutation Products in Structural Materials
Author(s) David Sprouster, J Trelewicz, D Morrall, X Hu, C Parish, B Wirth, Y Katoh, L Snead
On-Site Speaker (Planned) David Sprouster
Abstract Scope Structural materials in advanced fission and fusion reactors are exposed to extreme radiation conditions, that over time lead to the accumulation of transmutation products. These transmutation products have deleterious effects on the thermomechanical properties including severe toughness degradation and thermal conductivity decrease. Recent neutron irradiation experiments with mixed energy spectra have in fact demonstrated that refractory metals and alloys, in particular tungsten, are appreciably susceptible to the formation of nanometer-scale features involving transmutation products (Re and Os), which ultimately degrade the mechanical properties and rapid embrittlement at low irradiation doses. In this work, we employ multimodal synchrotron-based characterization methods to gain insights into the size, shape, and structure of transmutation products for a series of neutron irradiated tungsten specimens. The microstructural insights from the synchrotron characterization compliment modelling and electron microscopy results and shed new light on the size distributions and crystallographic phases of transmutation products that ensue after irradiation.
Proceedings Inclusion? Planned:
Keywords Characterization, Nuclear Materials,

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

4D X-ray Diffraction Microscopy Study of Tensile Deformation of Neutron-irradiated Fe-9Cr Alloy
Advanced Characterization of Nuclear Fuel Using Neutron Imaging
Characterization of Irradiated Nuclear Fuels with Pulsed Neutrons
Characterization of Long Range Ordering in Ni-based Alloys with Ex-situ and In-situ Synchrotron X-ray Diffraction
Characterization of Microstructure, Texture, And Residual Stress in a Neutron Irradiated CANDU Pressure Tube
Characterization of Nuclear Energy Materials in 2D and 3D using Laboratory-based X-ray Microscopy
Characterization of the Crystal Structure Evolution of U-Zr Alloys Utilizing Time-of-Flight Neutron Diffraction with In-situ-heating
Creep Behavior of Advanced Austenitic (Fe-25Ni-20Cr) Alloy 709 through In-situ Neutron Diffraction Characterization and Transmission Electron Microscopy Characterization
Evolution of Stresses in Deformation Twins in the Plastic Zone Using Three-dimensional Synchrotron X-ray Diffraction
Getting “Around” the High Mass Attenuation Issue for μX-ray Computed Tomography of Nuclear Fuels
Identifying the Microstructural Origins of Creep Damage in Alloy 617
In-situ Investigation into The Stability of Hydride Phases in Zirconium
In-situ Synchrotron X-ray Diffraction Study on Tensile Deformation of Neutron Irradiated Fe-Cr-C Alloys
In-Situ XRD Study of Alloy 709's Mechanical Behavior for Advanced Fast Reactor Applications
Irradiation-induced Effects in HT-UPS Steel Using Far-field X-ray Diffraction and Grain Tracking Analysis
Irradiation Effects on Precipitate Distributions in High-temperature Ultrafine-precipitate-strengthened Steel Characterized by Synchrotron Micro-computed Tomography
Microstructural Characterization of the Stress and Strain Deformation Partitioning Evolution in Tungsten Heavy Alloys
Microstructure and Crystal Structure Studies in the U-Zr System
Multimodal Synchrotron Characterization of Transmutation Products in Structural Materials
Neutron Imaging at LANSCE: Characterizing Nuclear Materials for Next Generation Reactor Designs.
Neutron Radiography Capabilities at LANSCE: Completing LANSCE's Cold/Thermal/Epithermal Imaging Suite With Fast-neutron Radiography
Non-destructive Characterization of Nuclear Materials using Neutron Imaging Techniques
Non-destructive Correlative 3D Characterization of Nuclear Graphite: From the Microscale to the Nanoscale
Synchrotron High-energy X-ray Studies of Nuclear Reactor Materials
Synchrotron Microdiffraction Study of Cracks and Indentation on UO2 Material
Transmission Spectrum Estimation and Material Decomposition with Energy Resolved Neutron Imaging
Using In-situ Synchrotron X-ray Scattering to Determine the TTT Diagram of U-6Nb
X-ray Based Nanodiffraction to Study Strain in Materials for Nuclear Energy

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